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蒸馏酒与配制酒卫生标准的分析方法蒸馏酒与配制酒卫生标准的分析方法 详细信息:
名称:填充柱
载体:GDX-102(60-80目),气相色谱用。或上试 402有机担体,60^-80目。
蒸馏酒与配制酒卫生标准的分析方法 测试谱图:
Analytical methods for the hygienic standards of distilled liquor and mixed liquor
Analytical methods for the hygienic standards of distilled spirits and blended spirits Details:
Name: Packed column
Carrier: GDX-102 (60-80 mesh) for gas chromatography. Or test 402 organic carrier, 60^-80 mesh.
Chromatographic column: length 2m, inner diameter 4mm, glass column or stainless steel column.
Application: GB/T 5009.48-1996 Analytical method of hygienic standards for distilled and mixed liquors
GB/T 5009.48-2003 Method for analysis of hygienic standards for distilled and mixed liquors
4.4 Methyl alcohol and higher alcohols (determined by gas chromatography)
441 Principle
The chemical io nization of different alcohols in a hydrogen flame is used for detection, and the peak height is compared with the standard. Minimum mark limit: Zheng Bing drunk, Zheng
Butanol 0.Zng, isoamyl alcohol, n-pentanol 0.15ng; seco ndary T alcohol, iso-T alcohol 0.22ng.
4.4.2 Reagents
4.4.3 Apparatus
44.3.1 Gas chromatograph: with hydrogen flame io nization detector.
4.4-3.2 Micro injection syringe: 1ul, 50ulL,
4.4.4 Analysis steps
4.4.4.1 Chromatographic reference conditions
4.4.4.1.1
Chromatographic column: length 2m, inner diameter 4mm, glass column or stainless steel column.
4.4.4.1.2
Statio nary phase: GDX-102,
60^-80 mesh. Or test 402 organic carrier, 60^-80 mesh.
4.4.4.1.3 Vaporization chamber temperature: 1900C,
4.4.4, .4 Detector temperature: 1900C,
4.4.4.1.5 Column temperature: 1700c,
4.4.4.1.6 Carrier gas (N2) flow rate: 40mL/min,
4.4.4.1.7 Hydrogen (H,) flow rate: 40mL/min,
4.4.4.1.8 Air flow rate: 450mL/min.
4.4.4., 9 Injection volume: 0.5ul
Analytical methods for the hygienic standards of distilled spirits and blended spirits Test spectrum:
色谱柱:长 2m,内径4mm,玻璃柱或不锈钢柱。
应用:GB/T 5009.48-1996 蒸馏酒与配制酒卫生标准的分析方法
GB/T 5009.48-2003 蒸馏酒与配制酒卫生标准的分析方法应用:GB/T 5009.48-1996 蒸馏酒与配制酒卫生标准的分析方法
4.4 甲醉和醇类(气相色谱法测定)
441 原理
利用不同醇类在氢火焰中的化学电离进行检测,根据峰高与标准比较定童。低标出限:正丙醉、正
丁醇0.Zng,异戊醇、正戊醉0.15ng;仲T醉、异T醇0.22ng。
4.4.2 试剂
4.4.3 仪器
44.3.1 气相色谱仪:具有氢火焰离子化检测器。
4.4-3.2 微量进样注射器:1ul,50ulL,
4.4.4 分析步骤
4.4.4.1 色谱参考条件
4.4.4.1.1
色谱柱:长 2m,内径4mm,玻璃柱或不锈钢柱。
4.4.4.1.2
固定相:GDX-102,
60^-80目。或上试 402有机担体,60^-80目。
4.4.4.1.3汽化室温度:1900C,
4.4.4,.4检测器温度:1900C,
4.4.4.1.5柱温:1700c,
4.4.4.1.6 载气(N2)流速:40mL/min,
4.4.4.1.7 氢气(H,)流速:40mL/min,
4.4.4.1.8 空气流速:450mL/min.
4.4.4.,,9 进样量:0.5ul
蒸馏酒与配制酒卫生标准的分析方法 测试谱图:
Analytical methods for the hygienic standards of distilled liquor and mixed liquor
Analytical methods for the hygienic standards of distilled spirits and blended spirits Details:
Name: Packed column
Carrier: GDX-102 (60-80 mesh) for gas chromatography. Or test 402 organic carrier, 60^-80 mesh.
Chromatographic column: length 2m, inner diameter 4mm, glass column or stainless steel column.
Application: GB/T 5009.48-1996 Analytical method of hygienic standards for distilled and mixed liquors
GB/T 5009.48-2003 Method for analysis of hygienic standards for distilled and mixed liquors
4.4 Methyl alcohol and higher alcohols (determined by gas chromatography)
441 Principle
The chemical io
Butanol 0.Zng, isoamyl alcohol, n-pentanol 0.15ng; seco
4.4.2 Reagents
4.4.3 Apparatus
44.3.1 Gas chromatograph: with hydrogen flame io
4.4-3.2 Micro injection syringe: 1ul, 50ulL,
4.4.4 Analysis steps
4.4.4.1 Chromatographic reference conditions
4.4.4.1.1
Chromatographic column: length 2m, inner diameter 4mm, glass column or stainless steel column.
4.4.4.1.2
Statio
60^-80 mesh. Or test 402 organic carrier, 60^-80 mesh.
4.4.4.1.3 Vaporization chamber temperature: 1900C,
4.4.4, .4 Detector temperature: 1900C,
4.4.4.1.5 Column temperature: 1700c,
4.4.4.1.6 Carrier gas (N2) flow rate: 40mL/min,
4.4.4.1.7 Hydrogen (H,) flow rate: 40mL/min,
4.4.4.1.8 Air flow rate: 450mL/min.
4.4.4., 9 Injection volume: 0.5ul
Analytical methods for the hygienic standards of distilled spirits and blended spirits Test spectrum: