安捷伦7890B玻璃柱Chromosorb 101 HP 60~80 气相色谱法测定医疗防护用品中环氧乙烷残留量
2022-01-28 19:56  点击:398
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气相色谱法测定医疗防护用品中环氧乙烷残留量
气相色谱法测定医疗防护用品中环氧乙烷残留量 详细信息:

安捷伦7890B玻璃柱
Chromosorb 101  HP 60~80目;玻璃柱长2m*3 mm

浩瀚色谱(山东)应用技术开发有限公司建立气相色谱法检测口罩、防护服等医疗防护用品中环氧乙烷的残留量,为生产厂家改进灭菌工艺提供数据支持。气相色谱法采用顶空进样、FID检测器,环氧乙烷的质量浓度在0.5~8 μg/mL范围内与色谱峰面积线性关系良好,检出限为0.10 μg/g,定量限为0.35 μg/g。环氧乙烷测定结果的相对标准偏差为1.73%(n=6),平均加标回收率为94.3%~99.3%。该方法操作简便,精密度、准确度较高,适用于医疗防护用品中环氧乙烷的测定。

气相色谱法测定医疗防护用品中环氧乙烷残留量 测试谱图:


Determination of ethylene oxide residues in medical protective equipment by gas chromatography
Determination of ethylene oxide residues in medical protective equipment by gas chromatography Details:

Agilent 7890B glass column
Chromosorb 101 HP 60~80 mesh; glass column length 2m*3 mm

Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has established a gas chromatography method to detect the residual amount of ethylene oxide in medical protective equipment such as masks and protective clothing, and provide data support for manufacturers to improve the sterilization process. Gas chromatography adopts headspace injection and FID detector. The mass concentration of ethylene oxide has a good linear relationship with the chromatographic peak area in the range of 0.5-8 μg/mL. The detection limit is 0.10 μg/g and the quantification limit is 0.35. μg/g. The relative standard deviation of the determination results of ethylene oxide was 1.73% (n=6), and the average recovery was 94.3%-99.3%. The method is easy to operate, has high precision and accuracy, and is suitable for the determination of ethylene oxide in medical protective equipment.

Determination of ethylene oxide residues in medical protective equipment by gas chromatography Test spectrum: 


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